HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → HCID 70240724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | SR142948A | HCID 5311451 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 70240724 | HCID 70240724 | 26.6% |
Reaction Steps
0.1 g of the compound obtained in EXAMPLE 1' is dissolved in 1.5 ml of EtOH and 1.5 ml of DCM, 0.015 g of diethanolamine is added and the mixture is left stirring for 30 minutes at RT and left overnight at 5° C. The crystallized product formed is drained. 0.03 g of the expected product is obtained, m.p. 200° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05936123 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-59f3c421ac714f0ea55f92db295df432 |
| Source note | uspto-grants-1999_08 |