HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethyl bromide → 2-Phenylethyl-p-toluenethiosulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | Benzenesulfonothioic acid, 4-methyl-, potassium salt (1:1) | HCID 23662126 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Phenylethyl-p-toluenethiosulfonate | HCID 86753003 | — |
Reaction Steps
The title compound was prepared according to General Method 2 using phenethyl bromide (0.088 mmol), potassium thiotosylate(0.088 mol), and absolute ethanol (250 mL). A clear liquid was obtained which was used without purification. 1H NMR (CDCl3) δ 2.47 (s, 3 H), 2.92 (t, 2 H), 3.24 (t, 2 H), 7.1-7.4 (m, 7 H), 7.84 (d, 2 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05936128 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-65eec409d84145fda298be22b642dda7 |
| Source note | uspto-grants-1999_08 |