HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 86023-87-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 82182-52-3 | HCID 255300 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 86023-87-2 | HCID 158910 | — |
Reaction Steps
(3β,5α,12β,25R)-3,12-di(acetoxy)-spirostan-11-one (purchased from Steraloids, Inc., or see preparation G13) was saponified with potassium carbonate in water, methanol and THF to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05939398 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-e60040b239454d60a937da484495555b |
| Source note | uspto-grants-1999_08 |