HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrofluoric Acid → HCID 22872555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrofluoric Acid | HCID 14917 | — |
| Reactant | HCID 53939621 | HCID 53939621 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 22872555 | HCID 22872555 | — |
Reaction Steps
Using the procedure described in J. Am. Chem. Soc., 1972, 94, 6190, (3β,5α,25R)-3-(t-butyldimethylsilyloxy)spirostan-11,12-dione was desilylated with hydrofluoric acid in acetonitrile to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05939398 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-7a6d8671eadb41afb02bc7b2c3d3ce71 |
| Source note | uspto-grants-1999_08 |