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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1585528Generated: November 1, 2026

Pyridine → HCID 53967493, compound

https://huagongshe.com/reaction/1585528

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
ReactantAcetic AnhydrideHCID 7918—
Reactant2-DimethylaminopyridineHCID 21885—
ReactantHCID 53796401HCID 53796401—
SolventDichloromethaneHCID 6344—
ProductHCID 53967493HCID 53967493—

Reaction Steps

(3β,5α,11β,12β,25R)-3-(t-butyldimethylsilyloxy)spirostan-11,12-diol was selectively acetylated with acetic anhydride, pyridine and dimethylaminopyridine in methylene chloride to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05939398
Source datasetuspto-grants-1999_08
ORD IDord-ed005bdbb38144ef854dfc7fee5590b4
Source noteuspto-grants-1999_08