HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-chloro-2-Methylphenoxy)acetic acid → (4-chloro-2-Methylphenoxy)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-chloro-2-Methylphenoxy)acetic acid | HCID 7204 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Product | (4-chloro-2-Methylphenoxy)acetic acid | HCID 7204 | — |
| Product | Potassium (4-chloro-2-methylphenoxy)acetate | HCID 23682017 | — |
Reaction Steps
6.6 parts (0.1 mol) of powdered potassium hydroxide (85%) are introduced into a melt of 20 parts (0.1 mol) of MCPA (93.3%) with stirring and the mixture is kept at 130° C. for 30 minutes. After solidification, 26 parts of MCPA-potassium having an MCPA content of 71.8% are obtained, which corresponds to a yield of 100%. M.p.: 203° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05939584 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-da9afdd0d8a24be3b24a8caa4d5f8bec |
| Source note | uspto-grants-1999_08 |