HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylhydroxylamine → N-Cyclohexyl-alpha-(2sulfofuran-5-yl)nitrone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylhydroxylamine | HCID 72935 | — |
| Reactant | 2-Formylfuran-5-sulfonate | HCID 2724001 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | N-Cyclohexyl-alpha-(2sulfofuran-5-yl)nitrone | HCID 85040086 | 84.3% |
Reaction Steps
Following the procedure of Example 1 above and using 5-formylfuran-2-sulfonic acid, sodium salt hydrate and N-cyclohexylhydroxylamine, the title compound was prepared in 84.3% yield as the sodium salt, m.p. 236.1° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05942507 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-cc4909ddb8d9475985e423f32cbf849b |
| Source note | uspto-grants-1999_08 |