HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sec-Butylamine → HCID 18789132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sec-Butylamine | HCID 24874 | — |
| Reactant | HCID 18789177 | HCID 18789177 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 18789132 | HCID 18789132 | 89% |
Reaction Steps
Synthesis was performed by the reaction of 5.26 g of 6-(2-chloroethyl)-5,7-dichloropyrazolo[1,5-a]pyrimidine with 4.00 g of sec-butylamine and 4.82 g of triethylamine in accordance with the synthetic process in Referential Example 9 to obtain 4.68 g (yield: 89.0%) of the intended product. White crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05942515 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-9deae11ff5774601a0ab23c01479043a |
| Source note | uspto-grants-1999_08 |