Methyl iodide → HCID 54713903, compound

HRID 1586084Notes

Reaction equation

HRID 1586084 reaction equation
[N+:1]([C:4]1[CH:13]=[C:12]2[C:7]([C:8]([OH:20])=[C:9]([O:16][C:17](=O)[CH3:18])[C:10](=[O:15])[N:11]2[CH3:14])=[CH:6][CH:5]=1)([O-:3])=[O:2].[CH2:21](Br)C=C.CI>>[N+:1]([C:4]1[CH:13]=[C:12]2[C:7]([C:8]([OH:20])=[C:9]([O:16][CH2:17][CH:18]=[CH2:21])[C:10](=[O:15])[N:11]2[CH3:14])=[CH:6][CH:5]=1)([O-:3])=[O:2]

Participants

4

Reactant 3

HCID 6328Methyl iodideHCID 7841Allyl bromideHCID 54713869HCID 54713869, compound

Product 1

HCID 54713903HCID 54713903, compound

Procedure

In accordance with EXAMPLE 15, using 7-nitro-3-acetoxy-4-hydroxy-1-methyl-2(1H)-quinolinone, allyl bromide was used as an alkylating agent instead of methyl iodide, 7-nitro-3-(2-propenyloxy)-4-hydroxy-1-methyl-2(1H)-quinolinone was provided. In the following, the spectrum data was shown.

Sources & evidence

ORD record
ord-6f75437fe3a14f539da9aa78c67b2acc
Source dataset
uspto-grants-1999_08
Patent number
US05942521

Reaction notes

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