Hydrochloric Acid → HCID 70066250, compound

Participants

Reaction Steps

Methyl 4-(aminoiminomethyl)-beta-[3-(aminoiminomethyl) phenyl]benzene pentanoate bis(trifluoroacetate) (0.030 gm, 0.08 mmol) was dissolved in 0.5 mL of 6 N HCl under N2 and stirred at room temperature for 48 hrs. The solution was concentrated to give the title compound as a white solid 0.018 gm (66%). Mp >200° C. (dec); MS: (M+H)+ 339; 1H NMR (DMSO-d6): 2.0 (m, 2H), 2.5 (m, 2H), 2.7 (dd, 1H), 2.85 (dd, 1H), 3.15(m, 1H), 7.40 (d, 2H), 7.55 (m, 2H), 7.75 (m, 4H), 9.1 (d, 4H), 9.25 (d, 4H).

Provenance & Evidence