HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azetidinecarboxylic Acid → AzeOH D-tartrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azetidinecarboxylic Acid | HCID 17288 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | D-Tartaric acid | HCID 439655 | — |
| Solvent | Water | HCID 962 | — |
| Product | AzeOH D-tartrate | HCID 131721350 | — |
Reaction Steps
The method described in Example 1 above was followed using DL-AzeOH (2.9 g; 29 mmol), D-tartaric acid (4.3 g; 29 mmol), 1,4-dioxane (5.5 g) and water (4.5 g) to yield 3.4 g (109%, as calculated from the theoretical yield) of L-AzeOH-D-tartrate with a d.e. of 73%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05942630 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-5d5b82a147df4312b7eea6c8f98f42a0 |
| Source note | uspto-grants-1999_08 |