1,8-Diaminonaphthalene → HCID 18785364, compound

Participants

Reaction Steps

With 1.58 g of 1,8-diaminonaphthalene, 10.8 g of diethyl ketone and 25 mg of sodium p-toluenesulfonate monohydrate were mixed. The mixture was heated and stirred for 5 hours in a steam bath. The resulting mixture was extracted with 100 ml of ethyl acetate and 50 ml of a saturated aqueous solution of sodium hydrogencarbonate. The solvent was distilled out to obtain 20 g of 2,2-diethyl-2,3-dihydroperimidine.

Provenance & Evidence