HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 21852618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 4-Nitroaniline | HCID 7475 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21852618 | HCID 21852618 | — |
Reaction Steps
To a solution of 1.38 g (0.01 mole) p-nitroaniline in 10 mL of acetone was added a solution of p-toluenesulfonic acid (2.375 g, 0.0125 mole) in 10 mL of acetone at room temperature. After stirring for 1 hour at room temperature, the reaction mixture was cooled to 5° C. and the product was isolated by filtration. The yield was 2.49 g (80% of theory) of a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05945374 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-2a385c9309184e879447669a966206fd |
| Source note | uspto-grants-1999_08 |