HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 2-[[(4-Methyl-1H-benzimidazol-2-yl)sulfinyl]methyl]benzenamine hemihydrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-[[(4-Methyl-1H-benzimidazol-2-yl)thio]methyl]benzenamine | HCID 14064649 | — |
| Product | 2-[[(4-Methyl-1H-benzimidazol-2-yl)sulfinyl]methyl]benzenamine hemihydrate | HCID 69796760 | — |
Reaction Steps
The title compound (740 mg) was prepared by the method of Example 3 using 900 mg of the title product of Example 7 instead of the title product of Example 2. Anal. Calc'd. for C15H15N3S*1/2 H2O: C, 61.20; H,5.48; N, 14.27; S, 10.89. Found: C, 61.21; H, 5.05; N, 13.88; S, 11.12.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05945425 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-827a4a6c8fb14756b2f1698f9808d720 |
| Source note | uspto-grants-1999_08 |