Diethyl Ether → HCID 69796367, compound

Participants

Reaction Steps

The title compound was prepared by the method of Example 3 using 950 mg of the title product of Example 29 instead of the title product of Example 2. Trituration with diethylether gave 434 mg of the title compound. Anal. Calc'd. for C16H17N3OS*1/2H2O: C, 62.23; H, 5.88; N, 13.63; S, 10.40. Found: C, 62.39; H, 5.72; N, 13.50; S, 10.65.

Provenance & Evidence