Water → HCID 178507579, compound

Participants

Reaction Steps

The title compound was prepared by the method of Example 85 using 350 mg of 6-[[[5-(hydroxymethyl)-1H-benzimidazol-2-yl]thio]methyl]-2-pyridinamine (see Example 104) instead of 6-[(1H-benzimidazol-2-yl)thiomethyl]-2-pyridinamine. Structure assignment was supported by the nmr and infrared spectra and by elemental analysis. Anal. Calc'd. for C14H14N4S02 *1/4 H2O: C, 54.80; H,4.60; N, 18.25; S, 10.44. Found: C, 54.85; H, 4.70; N, 18.01; S, 10.26.

Provenance & Evidence