HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Dimethyl benzylidenemalonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Dimethyl malonate | HCID 7943 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Dimethyl benzylidenemalonate | HCID 245906 | — |
Reaction Steps
Into a one-liter three-necked conical flask are introduced in succession 60 g (565.39 mmol) of benzaldehyde, 77 g of dimethyl malonate (565.32 mmol), 3.85 g of piperidine (45.21 mmol), 130 ml of toluene and 2.71 g (45.16 mmol) of acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05945548 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-6406b78e96124cb49e0643d60a77bb28 |
| Source note | uspto-grants-1999_08 |