HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzamide → HCID 354311, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzamide | HCID 1645 | — |
| Reactant | Anthranilamide | HCID 6942 | — |
| Reactant | 2-Methoxyethanol | HCID 8019 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | HCID 354311 | HCID 354311 | — |
Reaction Steps
10 g of 3-aminobenzamide and 30 g of rainy nickel were mixed with 150 ml of 2-methoxy ethanol and refluxed for 15 hours. (Molar ratio of aminobenzamide:solvent=1:26.) Celite was added to the reaction mixture and the debris removed by filtration. The filtrate was then evaporated under reduced pressure and the product, 3-(2-methoxyethylamino)benzamide crystallized on cooling, mp 89°-91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05215738 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-0c4e2b49102548bb8046a5497f0b803d |
| Source note | uspto-grants-1993_06 |