HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86746891, compound → HCID 86746890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86746891 | HCID 86746891 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86746890 | HCID 86746890 | 103.3% |
Reaction Steps
A mixture of 0.46 g (1.3 mmoles) of cis-2,3a-dibenzyl-3a,4,7,7a-tetrahydroisoindoline (Ex. 13), 0.46 g of platinum oxide and 100 mL of methanol were hydrogenated at 50 p.s.i. for 1 h. The catalyst was removed by filtration through celite and the filtrate was evaporated to give 0.41 g of the title compound as a clear oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05216018 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-3ac0fa65154d46cca4443a4b9ed498f5 |
| Source note | uspto-grants-1993_06 |