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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1586780Generated: October 31, 2026

HCID 86746891, compound → HCID 86746890, compound

https://huagongshe.com/reaction/1586780

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86746891HCID 86746891—
CatalystPlatinum oxide (PtO)HCID 82844—
SolventMethanolHCID 887—
ProductHCID 86746890HCID 86746890103.3%

Reaction Steps

A mixture of 0.46 g (1.3 mmoles) of cis-2,3a-dibenzyl-3a,4,7,7a-tetrahydroisoindoline (Ex. 13), 0.46 g of platinum oxide and 100 mL of methanol were hydrogenated at 50 p.s.i. for 1 h. The catalyst was removed by filtration through celite and the filtrate was evaporated to give 0.41 g of the title compound as a clear oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05216018
Source datasetuspto-grants-1993_06
ORD IDord-3ac0fa65154d46cca4443a4b9ed498f5
Source noteuspto-grants-1993_06