HCID 15067096, compound → HCID 15067079, compound

Participants

Reaction Steps

A total of 16 g of manganese dioxide is added in portions to a boiling solution of 8 g (40.6 mmol) of [2-(2-ethoxyethoxy)-5-pyridyl]-methanol in 200 ml of toluene within two hours. The mixture is then filtered hot and evaporated. Pale yellow oil, yield 7.1 g (90% of theory). 1H NMR (CDCl3 ; δ[ppm]): 1.2 (t, 3H); 3.6 (q, 2H); 3.8 (t, 2H); 4.6 (t, 2H); 6.9 (d, 1H); 8.1 (dd, 1H); 8.6 (d, 1H); 10.0 (s, 1H).

Provenance & Evidence