化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → 3-Methyl-1-(2-piperidinophenyl)-1-butylamine, (S)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | N-acetyl-L-glutamic acid | HCID 70914 | — |
| 反応物 | 3-Methyl-1-(2-piperidino-phenyl)-1-butylamine | HCID 10422052 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | 3-Methyl-1-(2-piperidinophenyl)-1-butylamine, (S)- | HCID 10514609 | — |
反応手順
Equimolar quantities of racemic 3-methyl-1-(2-piperidino-phenyl)-1-butylamine and of N-acetyl-L-glutamic acid were refluxed in aceton, whereby methanol was added in such an amount to yield a clear solution.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05216167 |
| 出典データセット | uspto-grants-1993_06 |
| ORD ID | ord-87c5e5558fd54e07848bb08cd8904b15 |
| 出典メモ | uspto-grants-1993_06 |