Ethanol → 2-Dimethylaminopyridine

HRID 1587588Notes

Reaction equation

[CH:1]1([N:7]=[C:8]=[N:9][CH:10]2[CH2:15][CH2:14][CH2:13]CC2)CCCCC1.[CH2:16](O)C>>[CH3:16][N:7]([C:8]1[CH:13]=[CH:14][CH:15]=[CH:10][N:9]=1)[CH3:1]

Participants

Reactant 2

HCID 702Ethanol

HCID 10868Dicyclohexylcarbodiimide

Product 1

HCID 218852-Dimethylaminopyridine

Procedure

Alternatively, a compound of the formula CXXI may be esterified by reaction with ethanol in the presence of dicyclohexylcarbodiimide and a catalyst such as dimethylaminopyridine to give a compound of the formula ##STR184##

Sources & evidence

ORD record: ord-77b90235a08146569ef1ff3d2a1f054b
Source dataset: uspto-grants-1993_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05217958

Reaction notes

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