HuagongsheHuagongshe Chemistry Print Report · For research reference only
1alpha,3beta-Bis(methoxycarbonyloxy)pregna-5,7-diene-20-carbaldehyde → 1alpha,3beta-Diacetoxy-20-methylpregna-5,7-diene-21-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1alpha,3beta-Bis(methoxycarbonyloxy)pregna-5,7-diene-20-carbaldehyde | HCID 54367523 | — |
| Reactant | 1alpha,3beta-Diacetoxypregna-5,7-diene-20-carbaldehyde | HCID 54379653 | — |
| Product | 1alpha,3beta-Diacetoxy-20-methylpregna-5,7-diene-21-ol | HCID 53906999 | 83.5% |
Reaction Steps
The procedure of Example 1 was repeated except that 93 mg of 1α,3β-diacetoxypregna-5,7-diene-20-carbaldehyde was used in lieu of 100 mg of 1α,3β-bis(methoxycarbonyloxy)pregna-5,7-diene-20-carbaldehyde to give 78 mg of 1α,3β-diacetoxy-20-methylpregna-5,7-diene-21-ol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05218109 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-36170db67f1545e6b7f6e780e421d63b |
| Source note | uspto-grants-1993_06 |