Potassium Carbonate → HCID 53934401, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 0.70 g of 1-(4-fluorophenyliminomethyl)-2-nitroiminoimidazolidine, 0.45 g of 2-chloro-5-chloromethylpyridine, 0.77 g of potassium carbonate and 5 ml of dimethylsulfoxide were agitated at 70° C. for 1 hour. The reaction mixture was, as it is, subjected to purification by column chromatography [silica gel, eluent: hexane-ethyl acetate (1:2)] to give 0.45 g of 1-(2-chloropyridin-5-ylmethyl)-2-nitroimino-3-(4-fluorophenyliminomethyl)imidazolidine.

Provenance & Evidence