HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 86746964, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 86746962 | HCID 86746962 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86746964 | HCID 86746964 | — |
Reaction Steps
1.13 g of 6-cyano-2-morpholinomethyl-8beta-ergoline-carboxylic acid methyl ester is dissolved in 45 ml of tetrahydrofuran and stirred with 2.4 ml of methyl iodide at room temperature overnight. The crystalline precipitate is filtered off, yield 1.26 g (82% of theory), [α]D =+9.7° (0.5% in DMSO).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05219862 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-8d85a33418be4c84916f93d26977ca32 |
| Source note | uspto-grants-1993_06 |