HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 86746970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 86746969 | HCID 86746969 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86746970 | HCID 86746970 | 83% |
Reaction Steps
161 mg of 6-cyano-8beta-methoxycarbonyl-2-ergoline-carbaldehyde (5 mmol) is dissolved in 10 ml of acetonitrile and reduced with 30 ml of sodium borohydride at room temperature in 1 hour. The solvent is largely evaporated, acidified with 2N hydrochloric acid and with addition of aqueous sodium bicarbonate solution the substance is obtained, yield 83%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05219862 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-c03e1781133f4ce3897c2732ef56f5cb |
| Source note | uspto-grants-1993_06 |