HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 15101055, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 1-Benzylpiperazine | HCID 75994 | — |
| Reactant | HCID 19756204 | HCID 19756204 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15101055 | HCID 15101055 | — |
Reaction Steps
A mixture of 3.8 g of 4-chloroacetyl-4,5-dihydro6-ethyl-7-[3-(trifluoromethyl)phenyl]pyrazolo[1,5-a]pyrimidine-3-carbonitrile, 1.8 ml of 1-benzyl piperazine and 1.1 g of sodium carbonate in 128 ml of toluene was reacted as described in Example 146, giving 3.7 g of the desired product, mp 97°-99° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05219857 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-6a8fa378cb764c8b906d65edd0606dd7 |
| Source note | uspto-grants-1993_06 |