HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Acetyl-3-nitrobenzamide → HCID 19756851, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Acetyl-3-nitrobenzamide | HCID 19756873 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19756851 | HCID 19756851 | — |
Reaction Steps
3-Nitro-N-(acetyl)phenylcarboxamide (200 mg) was dissolved in 60 ml of ethanol, treated with 200 mg of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 30 psi for 15 minutes. The reaction mixture was filtered through Celite and concentrated to give the title compound in quantitative yield as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05220018 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-45d592fa32ba4835900a3cf29d733928 |
| Source note | uspto-grants-1993_06 |