HCID 86745055, compound → HCID 178481964, compound

Participants

Reaction Steps

Aurous bis(tetramethylthiourea) tetrafluoroborate (0.201 g, prepared as described above) was dissolved in 3 mL methanol at room temperature and added dropwise to 1-methyl-4,5-diphenyl-1,2,4-triazolium-3-thiolate (0.216 g) which was partly dissolved in 3 mL methanol at room temperature. The mixture was stirred for 10 minutes after the addition was complete, and then a white powder was filtered (91% yield). This product was soluble in acetone. The elemental analysis conformed to the formula for compound 10.

Provenance & Evidence