Beta-Aminobutyric Acid → HCID 70072142, compound

HRID 1588092Notes

Reaction equation

HRID 1588092 reaction equation
[C:1]([C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][C:13]([OH:15])=O)=[CH:5][CH:4]=1)#[N:2].[CH3:16][CH:17]([CH2:19][C:20]([OH:22])=[O:21])[NH2:18].C1(C(CC(O)=O)[NH2:30])C=CC=CC=1>>[NH2:30][N:2]=[CH:1][C:3]1[CH:4]=[CH:5][C:6]([C:9]#[C:10][CH2:11][CH2:12][C:13]([NH:18][CH:17]([CH3:16])[CH2:19][C:20]([OH:22])=[O:21])=[O:15])=[CH:7][CH:8]=1

Participants

4

Reactant 3

HCID 10932Beta-Aminobutyric AcidHCID 69189DL-beta-PhenylalanineHCID 152807295-(4-Cyanophenyl)pentanoic acid

Product 1

HCID 70072142HCID 70072142, compound

Procedure

The title compound was prepared in the manner of Example 1 with the following modifications: Substituting 5-(p-cyanophenyl)-4-pentynoic acid for 5-(p-cyanophenyl)pentanoic acid and 3-methyl-beta-alanine for 3-phenyl-beta-alanine in procedure C of Example 1. The product was verified by C NMR (CD3OD) delta 15.5, 20.3, 34.5, 40.8, 42.0, 80.3, 92.2, 126.1, 127.8 131.2, 133.5, 166.7, 169.7, 172.5.

Sources & evidence

ORD record
ord-7f66270e73614284b8d1b3a600201844
Source dataset
uspto-grants-1993_06
Patent number
US05220050

Reaction notes

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