M-Cresol → HCID 67791463, compound

HRID 1588104Notes

Reaction equation

HRID 1588104 reaction equation
[OH-].[CH3:2][N+:3]([CH3:6])([CH3:5])[CH3:4].CO.[CH:9]1[C:14]([OH:15])=[CH:13][CH:12]=[CH:11][C:10]=1[CH3:16]>>[CH3:2][N+:3]([CH3:6])([CH3:5])[CH3:4].[CH:14]([OH:15])([CH3:9])[CH3:13].[CH3:16][C:10]1[CH:9]=[C:14]([O-:15])[CH:13]=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 342M-CresolHCID 19757443HCID 19757443, compound

Product 1

HCID 67791463HCID 67791463, compoundYield 200%

Procedure

To 5.40 ml of a commercially available 10% tetramethylammonium hydroxide-methanol solution (manufactured by TOKYO KASEI; 5.24 mmole equivalents) was added 0.566 g of m-cresol (5.24 mmoles), and about 7 ml of a tetramethylammonium-3-methylphenolate isopropanol solution (containing 5.24 mmoles of m-cresol) was obtained in the same manner as in Operation 1 in Example 4.

Sources & evidence

ORD record
ord-fbc16ff10ae2424999936595d39fef01
Source dataset
uspto-grants-1993_06
Patent number
US05220079

Reaction notes

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