Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(Trifluoromethyl)benzoyl chloride | HCID 75257 | — |
| Reactant | HCID 178508427 | HCID 178508427 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54572626 | HCID 54572626 | — |
Reaction Steps
In toluene (40 ml) were dissolved 2-imino-4,4-bis(trifluoromethyl)-5-(tetrafluoroethylidene)-1,3-thiazolidine (2.0 g) and triethylamine (1.0 ml), and a solution of 3-trifluoromethylbenzoyl chloride (1.5 g) dissolved in toluene (10 ml) was gradually added thereto under cooling and the mixture was stirred at 103° C. for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05221685 |
|---|
| Source dataset | uspto-grants-1993_06 |
|---|
| ORD ID | ord-35398c0994714c3488df43d5bcc56c3b |
|---|
| Source note | uspto-grants-1993_06 |
|---|
