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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1588290Generated: November 4, 2026

Triethylamine → HCID 53768479, compound

https://huagongshe.com/reaction/1588290

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
Reactant4-Fluorobenzoyl chlorideHCID 67879—
ReactantHCID 178508427HCID 178508427—
SolventTolueneHCID 1140—
ProductHCID 53768479HCID 53768479—

Reaction Conditions

Temperature103 °C

Reaction Steps

In toluene (40 ml) were dissolved 2-imino-4,4-bis(trifluoromethyl)-5-(tetrafluoroethylidene)-1,3-thiazolidine (2.0 g) and triethylamine (0.6 ml), and a solution of 4-fluorobenzoyl chloride (0.8 g) dissolved in toluene (10 ml) was gradually added thereto under cooling and the mixture was stirred at 103° C. for 3 hours.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05221685
Source datasetuspto-grants-1993_06
ORD IDord-500440819a1a4ff9a7f573559b32b11d
Source noteuspto-grants-1993_06