HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 2-(3-Trifluoromethoxybenzoylamino)-4,4-bis(trifluoromethyl)-5-(tetrafluoroethylidene)-2-thiazoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(Trifluoromethoxy)benzoyl chloride | HCID 522854 | — |
| Reactant | HCID 178508427 | HCID 178508427 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-(3-Trifluoromethoxybenzoylamino)-4,4-bis(trifluoromethyl)-5-(tetrafluoroethylidene)-2-thiazoline | HCID 54460595 | — |
Reaction Conditions
| Temperature | 103 °C |
|---|
Reaction Steps
In toluene (10 ml) were dissolved 2-imino-4,4-bis(trifluoromethyl)-5-(tetrafluoroethylidene)-1,3-thiazolidine (1.0 g) and triethylamine (0.6 ml), and a solution of 3-trifluoromethoxybenzoyl chloride (0.5 g) dissolved in toluene (10 ml) was gradually added thereto under cooling and the mixture was stirred at 103° C. for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05221685 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-01f82ed9349a46e7af2c259011a50807 |
| Source note | uspto-grants-1993_06 |