2-Nitrobenzoyl isocyanate → HCID 53773282, compound

HRID 1588297Notes

Reaction equation

HRID 1588297 reaction equation
[NH:1]=[C:2]1[NH:6][C:5]([C:11]([F:14])([F:13])[F:12])([C:7]([F:10])([F:9])[F:8])[C:4](=[C:15]([F:20])[C:16]([F:19])([F:18])[F:17])[S:3]1.[N+:21]([C:24]1[CH:34]=[CH:33][CH:32]=[CH:31][C:25]=1[C:26]([N:28]=[C:29]=[O:30])=[O:27])([O-:23])=[O:22]>C1(C)C=CC=CC=1>[F:14][C:11]([F:12])([F:13])[C:5]1([C:7]([F:10])([F:9])[F:8])[C:4](=[C:15]([F:20])[C:16]([F:17])([F:18])[F:19])[S:3][C:2]([NH:1][C:29]([NH:28][C:26](=[O:27])[C:25]2[CH:31]=[CH:32][CH:33]=[CH:34][C:24]=2[N+:21]([O-:23])=[O:22])=[O:30])=[N:6]1

Participants

4

Reactant 2

HCID 125834382-Nitrobenzoyl isocyanateHCID 178508427HCID 178508427, compound

Product 1

HCID 53773282HCID 53773282, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

In toluene (10 ml) was dissolved 2-imino-4,4-bis(trifluoromethyl)-5-(tetrafluoroethylidene)-1,3-thiazolidine (1.0 g), and 2-nitrobenzoylisocyanate (0.4 g) which is a starting compound was added thereto and the mixture was stirred at room temperature for 3 hours.

Workup

  1. additionwas added

Sources & evidence

ORD record
ord-33d1643ec39d4d6baeffcb3266b7547e
Source dataset
uspto-grants-1993_06
Patent number
US05221685

Reaction notes

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