Hydrazine → HCID 15599439, compound

HRID 1588336Notes

Reaction equation

HRID 1588336 reaction equation
[CH3:1][N:2]1[C:7]2[CH:8]=[CH:9][C:10]([C:12](=O)[CH:13]([CH3:19])[CH2:14][C:15](OC)=[O:16])=[CH:11][C:6]=2[O:5][CH2:4][C:3]1=[O:21].[NH2:22][NH2:23]>>[CH3:1][N:2]1[C:7]2[CH:8]=[CH:9][C:10]([C:12]3[CH:13]([CH3:19])[CH2:14][C:15](=[O:16])[NH:22][N:23]=3)=[CH:11][C:6]=2[O:5][CH2:4][C:3]1=[O:21]

Participants

3

Reactant 2

HCID 9321HydrazineHCID 15035920HCID 15035920, compound

Product 1

HCID 15599439HCID 15599439, compound

Procedure

Methyl 4-(3,4-dihydro-4-methyl-3-oxo-1,4(2H)-benzoxazin-7-yl)-4-oxo-3-methylbutyrate was treated with hydrazine as in example 1 to give the title compound, mp 188°-190° C.

Sources & evidence

ORD record
ord-6b0237c365d740db991073390574e646
Source dataset
uspto-grants-1993_06
Patent number
US05221742

Reaction notes

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