HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 131718005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 131718003 | HCID 131718003 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 131718005 | HCID 131718005 | 72% |
Reaction Steps
Tetrabutylammonium fluoride (1.0M in THF, 3.95 ml) was added to a solution of the monoalcohol (40) (0.479 g) in THF and the mixture was stirred overnight at room temperature. The crude product obtained after the usual work-up was subjected to silicagel column chromatography to give the diol (41).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05221799 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-d60c88ed5a7f422784581442e62bf97f |
| Source note | uspto-grants-1993_06 |