HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Isooctylacrylate Acrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | 2,2'-Azobis(2,4-dimethylvaleronitrile) | HCID 91537 | — |
| Reactant | Isooctyl acrylate | HCID 165746 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | Ethylacetate methanol | HCID 21584119 | — |
| Product | Isooctylacrylate Acrylamide | HCID 6452299 | — |
Reaction Steps
The procedures above were repeated this time employing 782.55 g of isooctyl acrylate, 49.95 g of acrylamide, 1.665 g of 2,2'-azobis(2,4-dimethylpentanenitrile), 1275.75 g of ethyl acetate and 141.75 g of methanol. The resulting copolymer was diluted with ethyl acetate/methanol (90/10) to 26.86% solids and had a measured inherent viscosity of 1.00 dl/g in ethyl acetate at a concentration of 0.15 g/dl. The Brookfield viscosity was 2,320 centipoise.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223261 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-c32d6b1c9cda4208b5424bc4cd0d8e91 |
| Source note | uspto-grants-1993_06 |