HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propionitrile → HCID 178458050, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propionitrile | HCID 7854 | — |
| Reactant | 2-Morpholinoaniline | HCID 735756 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | HCID 178458050 | HCID 178458050 | — |
Reaction Steps
A mixture of 4-(2-aminophenyl)morpholine (5.34 g), propionitrile (4.7 g) and anhydrous aluminium chloride (12 g) was heated at 160°-170° C. for six hours to yield N-(2-morpholinophenyl)propionamidine (m.p. 114° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223498 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-5c68fd2bd4054f52a359be43bf0c1e55 |
| Source note | uspto-grants-1993_06 |