HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 15746509, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 18952334 | HCID 18952334 | — |
| Product | HCID 15746509 | HCID 15746509 | — |
Reaction Steps
Reaction of 6-methyl-2-morpholinophenyl isothiocyanate (8.8 g) with 33% alcoholic ammonia solution (60 ml) at room temperature for 5 hours gave 1-(6-methyl-2-morpholinophenyl)thiourea (9 g) as a pale yellow solid, m.p. 199° C. which was recrystallised from a 1:1 mixture of ethylacetate and hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223498 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-2e8b1dcedff64c59938c43f191e30215 |
| Source note | uspto-grants-1993_06 |