Ammonia → HCID 18952152, compound

HRID 1588627Notes

Reaction equation

[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([N:11]2[CH2:16][CH2:15][O:14][CH2:13][CH2:12]2)=[C:6]([N:8]=[C:9]=[S:10])[CH:7]=1.[NH3:17]>>[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([N:11]2[CH2:16][CH2:15][O:14][CH2:13][CH2:12]2)=[C:6]([NH:8][C:9]([NH2:17])=[S:10])[CH:7]=1

Participants

Reactant 2

HCID 222Ammonia

HCID 18952186HCID 18952186, compound

Product 1

HCID 18952152HCID 18952152, compound

Procedure

Reaction of 5-methyl-2-morpholinophenyl isothiocyanate (15 g) with 33% ethanolic ammonia solution for 48 hours at room temperature gave 1-(5-methyl-2-morpholinophenyl)thiourea as a pale yellow solid (m.p. 181°-182° C.).

Sources & evidence

ORD record: ord-3078cc210a504c7687cab09c575eabf9
Source dataset: uspto-grants-1993_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05223498

Reaction notes

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