HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 18952330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 8625259 | HCID 8625259 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 18952330 | HCID 18952330 | — |
Reaction Steps
A mixture of 1-ethyl-3-(2-morpholinophenyl) thiourea (3.2 g) and methyliodide (2 g) in acetone (25 ml) was heated at reflux for 4 hours to yield 2-methyl-3-ethyl-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide as a pale yellow solid (m.p. 170°-172° C. which was recrystallised from acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223498 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-8157ce41150b44c8b32132d0b6ebed50 |
| Source note | uspto-grants-1993_06 |