HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 1-(5-Chloro-2-morpholinophenyl)thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 5-Chloro-2-morpholinophenyl isothiocyanate | HCID 18952098 | — |
| Product | 1-(5-Chloro-2-morpholinophenyl)thiourea | HCID 18952243 | — |
Reaction Steps
Reaction of 5-chloro-2-morpholinophenyl isothiocyanate (10 g) with 33% alcoholic ammonia solution (60 ml) at room temperature for 14 hours gave 1-(5-chloro-2-morpholinophenyl)thiourea as a yellow solid (m.p. 174°-175° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223498 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-7becbf93c1af44f0bd6871e1b948fd45 |
| Source note | uspto-grants-1993_06 |