HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthoic acid → HCID 14880508, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthoic acid | HCID 7123 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 14880491 | HCID 14880491 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 14880508 | HCID 14880508 | 59.5% |
Reaction Steps
Working in a manner similar to that described in Example 9, but starting with 2-naphthalenecarboxylic acid (0.95 g), oxalyl dichloride (0.7 g), 2-amino-N,N-diphenylacetamide (1.2 g) and triethylamine (0.8 g), and after recrystallization in acetonitrile, N-(diphenylcarbamoylmethyl)-2-naphthalenecarboxamide (1.2 g), m.p. 205° C., is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223529 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-8f0f9a96ba9b4487ba54a34f564b230c |
| Source note | uspto-grants-1993_06 |