Methanol → HCID 19755043, compound

HRID 1588950Notes

Reaction equation

HRID 1588950 reaction equation
[CH3:1][C:2]1[NH:6][CH:5]=[N:4][C:3]=1[CH2:7][N:8]1C[CH2:23][CH2:22][C:11]2[N:12]3[C:21]4[C:16](=[CH:17][CH:18]=[CH:19][C:20]=4[C:10]=2[C:9]1=[O:25])[CH2:15][CH2:14][CH2:13]3.[CH3:26]O>>[CH3:1][C:2]1[NH:6][CH:5]=[N:4][C:3]=1[CH2:7][N:8]1[CH2:23][CH2:22][C:11]2[N:12]3[C:21]4[C:20](=[CH:19][CH:18]=[CH:17][C:16]=4[CH2:15][CH2:14][CH2:26][CH2:13]3)[C:10]=2[C:9]1=[O:25]

Participants

3

Reactant 2

HCID 887MethanolHCID 54546622HCID 54546622, compound

Product 1

HCID 19755043HCID 19755043, compound

Procedure

11-{(5-methyl-1H-imidazol-4-yl)methyl}-5,6,9,10,11,12-hexahydro-4H, 8H-azepino[3',4':4,5] pyrrolo[3,2,1-ij]quinolin-12-one; melting point 215°-216° C. C-13-NMR (SLV: CDCl3, Ref.: TMS, ADT: MeOH)

Sources & evidence

ORD record
ord-8dead9ed17354a16add90f246a3fb1a8
Source dataset
uspto-grants-1993_06
Patent number
US05223625

Reaction notes

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