N-(3-Chlorophenyl)-2-[[(3,4-dimethoxyphenyl)methyl]amino]acetamide → N-(3-chlorophenyl)-N'-[(3,4-dimethoxyphenyl)methyl]-1,2-ethanediamine

Participants

Role	Name	HCID	Charge
Reactant	N-(3-Chlorophenyl)-2-[[(3,4-dimethoxyphenyl)methyl]amino]acetamide	HCID 14998797	—
Reactant	Aluminium lithium hydride	HCID 21226445	—
Product	N-(3-chlorophenyl)-N'-[(3,4-dimethoxyphenyl)methyl]-1,2-ethanediamine	HCID 14998759	—

Reaction Steps

In a manner similar to Preparation 2, react N-(3-chlorophenyl)-2-[[(3,4-dimethoxyphenyl)methyl]amino]acetamide (13.6 g, 40.1 mmol) with lithium aluminum hydride (3.1 g, 81 mmol) to obtain the title compound.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US05223623
Source dataset	uspto-grants-1993_06
ORD ID	ord-b532a3de67f84d28b74cb7a6cf6f18f2
Source note	uspto-grants-1993_06