Sodium Acetate → HCID 178460147, compound

HRID 1589100Notes

Reaction equation

HRID 1589100 reaction equation
[C:1]([CH:6]1[C:11](=[O:12])[CH2:10][CH:9]([C:13]2[C:18]([CH3:20])([CH3:19])[CH2:17][CH2:16][CH2:15][C:14]=2[CH3:21])[CH2:8][C:7]1=[O:22])(=O)[CH2:2][CH2:3][CH3:4].[Cl-].[CH2:24]([O:27][NH3+:28])[CH:25]=[CH2:26].C([O-])(=O)C.[Na+]>C(O)C>[CH2:24]([O:27][NH:28][C:1](=[C:6]1[C:7](=[O:22])[CH2:8][CH:9]([C:13]2[C:18]([CH3:20])([CH3:19])[CH2:17][CH2:16][CH2:15][C:14]=2[CH3:21])[CH2:10][C:11]1=[O:12])[CH2:2][CH2:3][CH3:4])[CH:25]=[CH2:26]

Participants

5

Reactant 3

HCID 517045Sodium AcetateHCID 13044540HCID 13044540, compoundHCID 13589694HCID 13589694, compound

Product 1

HCID 178460147HCID 178460147, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

8.0 parts by weight of 2-butyryl-5-(1,3,3-trimethylcyclohex-1-en-2-yl)-cyclohexane-1,3-dione are reacted with 2.9 parts by weight of allyloxyammonium chloride and 2.4 parts by weight of sodium acetate in 100 parts by volume of ethanol and the mixture is worked up, by a procedure similar to that of Example 1. 9.0 parts by weight of 2-(1-allyloxyaminobutylidene)-5-(1,3,3-trimethylcyclohex-1-en-2-yl)-cyclohexane-1,3-dione are obtained as a viscous oil (active ingredient No.2).

Sources & evidence

ORD record
ord-62e44a79a9b54348a0b7f7a333300f31
Source dataset
uspto-grants-1986_02
Patent number
US04568383

Reaction notes

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