HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 23720642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Fluorine | HCID 24524 | — |
| Reactant | Potassium perfluorooctanoate | HCID 4253803 | — |
| Solvent | Perfluoro-2-butyltetrahydrofuran | HCID 78976 | — |
| Product | HCID 23720642 | HCID 23720642 | — |
Reaction Steps
Potassium perfluorooctanoate (6 g) was stored in a desiccator over water for 3 days. After this period, the increased weight of the salt indicated the formation of the 1.0-1.5 hydrate. The hydrated salt was fluorinated in perfluoro-2-butyltetrahydrofuran with 1% fluorine in nitrogen until a solution containing 2.5 to 3 meq/l of fluoroxy compounds was formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04568478 |
| Source dataset | uspto-grants-1986_02 |
| ORD ID | ord-e6e329706af5451084da709c08f994de |
| Source note | uspto-grants-1986_02 |