HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Isatoic Anhydride → 2-amino-N-(3-imidazol-1-ylpropyl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Isatoic Anhydride | HCID 8359 | — |
| Edukt | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 2-amino-N-(3-imidazol-1-ylpropyl)benzamide | HCID 2798335 | — |
Reaktionsschritte
A mixture of 2.5 ml. of 1H-imidazole-1-propanamine, 3.2 g. of isatoic anhydride, and 30 ml. of toluene was heated at 90°-100° C. for 45 minutes and cooled. The precipitate which separated was collected by filtration. The desired product melted at 107°-110° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04568687 |
| Quelldatensatz | uspto-grants-1986_02 |
| ORD ID | ord-428fd3b689194c34a7656ed34fefaf49 |
| Quellennotiz | uspto-grants-1986_02 |