HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butyl hypochlorite → 1,1-Di(p-fluorophenyl)-3-chlorourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butyl hypochlorite | HCID 521297 | — |
| Reactant | 1,1-Di(p-fluorophenyl)urea | HCID 13362430 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1,1-Di(p-fluorophenyl)-3-chlorourea | HCID 20184152 | — |
Reaction Steps
t-Butyl hypochlorite (22.8 g, 0.21 mole) was added to 1,1-di(p-fluorophenyl)urea (49.4 g, 0.2 mole) in 750 ml methanol at 0°-5° and the mixture stirred for 0.5 hour to produce a thin slurry containing step (a) title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04568748 |
| Source dataset | uspto-grants-1986_02 |
| ORD ID | ord-6ee7e69bc25c4595bdd8c463cb59c9d2 |
| Source note | uspto-grants-1986_02 |